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{
"DOI" : "10.26850/1678-4618eqj.v35.1.2010.p41-46" ,
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2018 ,
1 ,
15
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"abstract" : "<jats:p>A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drugand in pharmaceutical preparations is proposed. The formation of a reddish-violet\u00a0 color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian\u00a0 Pharmacopoeia, using the Student\u2019s t and the F tests. Considering the concentration in a 100 \u03bcL aliquot, the qualitative visual limit of detection is about 5\u00d710-6 g; instrumental LOD \u2245 1.4\u00d710-4 mol L-1 ; LOQ \u2245 4.5\u00d710-4 mol L-1.</jats:p>" ,
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"given" : "A. C." ,
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"given" : "Marta Maria Duarte Carvalho" ,
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{
"authenticated-orcid" : false ,
"given" : "Leonardo" ,
"family" : "Pezza" ,
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"ORCID" : "http://orcid.org/0000-0003-0197-7369"
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{
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"given" : "Helena Redigolo" ,
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"ORCID" : "http://orcid.org/0000-0001-5564-1639"
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} ,
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"given" : "Matthieu" ,
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"ORCID" : "http://orcid.org/0000-0002-1987-3907"
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}
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"URL" : "http://dx.doi.org/10.26850/1678-4618eqj.v35.1.2010.p41-46" ,
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"Eclet. Quim. J."
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"title" : [
"Spot-test identification and rapid quantitative sequential analys is of dipyrone"
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"Ecl\u00e9tica Qu\u00edmica Journal"
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"page" : "41-50" ,
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