175 lines
4.2 KiB
JSON
175 lines
4.2 KiB
JSON
{
|
|
"DOI": "10.26850/1678-4618EQJ.v35.1.2010.p41-46",
|
|
"issued": {
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
1,
|
|
15
|
|
]
|
|
]
|
|
},
|
|
"abstract": "<jats:p>A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drugand in pharmaceutical preparations is proposed. The formation of a reddish-violet\u00a0 color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian\u00a0 Pharmacopoeia, using the Student\u2019s t and the F tests. Considering the concentration in a 100 \u03bcL aliquot, the qualitative visual limit of detection is about 5\u00d710-6 g; instrumental LOD \u2245 1.4\u00d710-4 mol L-1 ; LOQ \u2245 4.5\u00d710-4 mol L-1.</jats:p>",
|
|
"prefix": "10.26850",
|
|
"author": [
|
|
{
|
|
"authenticated-orcid": false,
|
|
"given": "Matthieu",
|
|
"family": "Tubino",
|
|
"sequence": "first",
|
|
"affiliation": [],
|
|
"ORCID": "http://orcid.org/0000-0002-1987-3907"
|
|
},
|
|
{
|
|
"affiliation": [],
|
|
"given": "A. C.",
|
|
"family": "Biondo",
|
|
"sequence": "additional"
|
|
},
|
|
{
|
|
"authenticated-orcid": false,
|
|
"given": "Marta Maria Duarte Carvalho",
|
|
"family": "Vila",
|
|
"sequence": "additional",
|
|
"affiliation": [],
|
|
"ORCID": "http://orcid.org/0000-0002-0198-7076"
|
|
},
|
|
{
|
|
"authenticated-orcid": false,
|
|
"given": "Leonardo",
|
|
"family": "Pezza",
|
|
"sequence": "additional",
|
|
"affiliation": [],
|
|
"ORCID": "http://orcid.org/0000-0003-0197-7369"
|
|
},
|
|
{
|
|
"authenticated-orcid": false,
|
|
"given": "Helena Redigolo",
|
|
"family": "Pezza",
|
|
"sequence": "additional",
|
|
"affiliation": [],
|
|
"ORCID": "http://orcid.org/0000-0001-5564-1639"
|
|
}
|
|
],
|
|
"reference-count": 0,
|
|
"ISSN": [
|
|
"1678-4618"
|
|
],
|
|
"member": "11395",
|
|
"source": "Crossref",
|
|
"score": 1.0,
|
|
"deposited": {
|
|
"timestamp": 1540823529000,
|
|
"date-time": "2018-10-29T14:32:09Z",
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
10,
|
|
29
|
|
]
|
|
]
|
|
},
|
|
"indexed": {
|
|
"timestamp": 1540825815212,
|
|
"date-time": "2018-10-29T15:10:15Z",
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
10,
|
|
29
|
|
]
|
|
]
|
|
},
|
|
"type": "journal-article",
|
|
"published-online": {
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
1,
|
|
15
|
|
]
|
|
]
|
|
},
|
|
"URL": "http://dx.doi.org/10.26850/1678-4618eqj.v35.1.2010.p41-46",
|
|
"is-referenced-by-count": 0,
|
|
"volume": "35",
|
|
"issn-type": [
|
|
{
|
|
"type": "electronic",
|
|
"value": "1678-4618"
|
|
}
|
|
],
|
|
"link": [
|
|
{
|
|
"URL": "http://revista.iq.unesp.br/ojs/index.php/ecletica/article/viewFile/191/149",
|
|
"intended-application": "text-mining",
|
|
"content-version": "vor",
|
|
"content-type": "application/pdf"
|
|
},
|
|
{
|
|
"URL": "http://revista.iq.unesp.br/ojs/index.php/ecletica/article/viewFile/191/149",
|
|
"intended-application": "similarity-checking",
|
|
"content-version": "vor",
|
|
"content-type": "unspecified"
|
|
}
|
|
],
|
|
"journal-issue": {
|
|
"issue": "1",
|
|
"published-online": {
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
1,
|
|
15
|
|
]
|
|
]
|
|
}
|
|
},
|
|
"references-count": 0,
|
|
"short-container-title": [
|
|
"Eclet. Quim. J."
|
|
],
|
|
"publisher": "Ecletica Quimica Journal",
|
|
"content-domain": {
|
|
"domain": [],
|
|
"crossmark-restriction": false
|
|
},
|
|
"license": [
|
|
{
|
|
"URL": "http://creativecommons.org/licenses/by/4.0",
|
|
"start": {
|
|
"timestamp": 1515974400000,
|
|
"date-time": "2018-01-15T00:00:00Z",
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
1,
|
|
15
|
|
]
|
|
]
|
|
},
|
|
"content-version": "unspecified",
|
|
"delay-in-days": 0
|
|
}
|
|
],
|
|
"created": {
|
|
"timestamp": 1517590842000,
|
|
"date-time": "2018-02-02T17:00:42Z",
|
|
"date-parts": [
|
|
[
|
|
2018,
|
|
2,
|
|
2
|
|
]
|
|
]
|
|
},
|
|
"issue": "1",
|
|
"title": [
|
|
"Spot-test identification and rapid quantitative sequential analys is of dipyrone"
|
|
],
|
|
"container-title": [
|
|
"Ecl\u00e9tica Qu\u00edmica Journal"
|
|
],
|
|
%s
|
|
"page": "41-50"
|
|
} |