175 lines
4.3 KiB
JSON
175 lines
4.3 KiB
JSON
{
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"DOI": "10.26850/1678-4618eqj.v35.1.2010.p41-46",
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"issued": {
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"date-parts": [
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[
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2018,
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1,
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15
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]
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]
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},
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"abstract": "<jats:p>A qualitative spot-test and tandem quantitative analysis of dipyrone in the bulk drugand in pharmaceutical preparations is proposed. The formation of a reddish-violet\u00a0 color indicates a positive result. In sequence a quantitative procedure can be performed in the same flask. The quantitative results obtained were statistically compared with those obtained with the method indicated by the Brazilian\u00a0 Pharmacopoeia, using the Student\u2019s t and the F tests. Considering the concentration in a 100 \u03bcL aliquot, the qualitative visual limit of detection is about 5\u00d710-6 g; instrumental LOD \u2245 1.4\u00d710-4 mol L-1 ; LOQ \u2245 4.5\u00d710-4 mol L-1.</jats:p>",
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"prefix": "10.26850",
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"author": [
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{
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"affiliation": [],
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"given": "A. C.",
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"family": "Biondo",
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"sequence": "additional"
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},
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{
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"authenticated-orcid": false,
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"given": "Marta Maria Duarte Carvalho",
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"family": "Vila",
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"sequence": "additional",
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"affiliation": [],
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"ORCID": "http://orcid.org/0000-0002-0198-7076"
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},
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{
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"authenticated-orcid": false,
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"given": "Leonardo",
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"family": "Pezza",
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"sequence": "additional",
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"affiliation": [],
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"ORCID": "http://orcid.org/0000-0003-0197-7369"
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},
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{
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"authenticated-orcid": false,
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"given": "Helena Redigolo",
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"family": "Pezza",
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"sequence": "additional",
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"affiliation": [],
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"ORCID": "http://orcid.org/0000-0001-5564-1639"
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},
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{
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"authenticated-orcid": false,
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"given": "Matthieu",
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"family": "Tubino",
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"sequence": "first",
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"affiliation": [],
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"ORCID": "http://orcid.org/0000-0002-1987-3907"
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}
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],
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"reference-count": 0,
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"ISSN": [
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"1678-4618"
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],
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"member": "11395",
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"source": "Crossref",
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"score": 1.0,
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"deposited": {
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"timestamp": 1540823529000,
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"date-time": "2018-10-29T14:32:09Z",
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"date-parts": [
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2018,
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10,
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29
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"indexed": {
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"timestamp": 1540825815212,
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"date-time": "2018-10-29T15:10:15Z",
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2018,
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},
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"type": "journal-article",
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"published-online": {
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2018,
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1,
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},
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"URL": "http://dx.doi.org/10.26850/1678-4618eqj.v35.1.2010.p41-46",
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"is-referenced-by-count": 0,
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"volume": "35",
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"issn-type": [
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{
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"type": "electronic",
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"value": "1678-4618"
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}
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],
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"link": [
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{
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"URL": "http://revista.iq.unesp.br/ojs/index.php/ecletica/article/viewFile/191/149",
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"intended-application": "text-mining",
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"content-version": "vor",
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"content-type": "application/pdf"
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{
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"URL": "http://revista.iq.unesp.br/ojs/index.php/ecletica/article/viewFile/191/149",
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"intended-application": "similarity-checking",
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"content-version": "vor",
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"content-type": "unspecified"
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],
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"journal-issue": {
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"issue": "1",
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}
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},
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"references-count": 0,
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"short-container-title": [
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"Eclet. Quim. J."
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],
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"publisher": "Ecletica Quimica Journal",
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"content-domain": {
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"domain": [],
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"crossmark-restriction": false
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},
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"license": [
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{
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"URL": "http://creativecommons.org/licenses/by/4.0",
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"start": {
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"timestamp": 1515974400000,
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"date-time": "2018-01-15T00:00:00Z",
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"content-version": "unspecified",
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"created": {
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"timestamp": 1517590842000,
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"date-time": "2018-02-02T17:00:42Z",
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2
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},
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"issue": "1",
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"title": [
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"Spot-test identification and rapid quantitative sequential analys is of dipyrone"
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],
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"container-title": [
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"Ecl\u00e9tica Qu\u00edmica Journal"
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],
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"page": "41-50",
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"funder": [{"DOI": "10.13039/100010663","name": "H2020 European Research Council","doi-asserted-by": "publisher","award": ["677749"]}]
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} |